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Corrections to "An Optimized Safe Process from Bench to Pilot cGMP Production of API Eptifibatide Using a Multigram-Scale Microwave-Assisted Solid-Phase Peptide Synthesizer".
D'Ercole A, Pacini L, Sabatino G, Zini M, Milli L, Nuti F, Ribecai A, Paio A, Rovero P, Papini AM. D'Ercole A, et al. Among authors: ribecai a. Org Process Res Dev. 2022 Aug 19;26(8):2540. doi: 10.1021/acs.oprd.2c00224. Epub 2022 Jul 29. Org Process Res Dev. 2022. PMID: 36037038 Free PMC article.
A multi-technique approach using LC-NMR, LC-MS, semi-preparative HPLC, HR-NMR and HR-MS for the isolation and characterization of low-level unknown impurities in GW876008, a novel corticotropin-release factor 1 antagonist.
Provera S, Rovatti L, Turco L, Mozzo S, Spezzaferri A, Bacchi S, Ribecai A, Guelfi S, Mingardi A, Marchioro C, Papini D. Provera S, et al. Among authors: ribecai a. J Pharm Biomed Anal. 2010 Nov 2;53(3):517-25. doi: 10.1016/j.jpba.2010.06.012. Epub 2010 Jun 22. J Pharm Biomed Anal. 2010. PMID: 20619567